Motorola LS6000B-U Guía de usuario Pagina 125
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LS 6000 Scintillation System User’s Manual
PN 247971-F
6-23
Isotope/DPM Libraries
Setting Up A Quench Curve
6
1. From the Main Menu, highlight “Isotope/DPM Libraries” and press SELECT. The Main
Editing Window displays two prompts: Setup and Review Isotopes and Setup and
Review DPM Quench Curves.
2. Highlight “Set Up and Review DPM Quench Curves” and press SELECT. The Main
Editing Window displays two prompts: Normal Quench Curves and Low Level Quench
Curves.
3. Highlight “Normal Quench Curves” if the quench curve to delete is stored in the
Standard DPM Library. Highlight “Low Level Quench Curves” if the quench curve to
delete is stored in the Low Level DPM Library. Press SELECT. The Main Editing
Window displays two prompts: Setup Quench Curves and Review/Edit/Delete Quench
Curves.
4. Highlight “Review/Edit/Delete Quench Curves” and press SELECT. The menu shown in
Figure 6.14 is displayed.
5. Highlight “Select Quench Curve” and choose the quench curve to delete.
6. Before you delete a quench curve, you may want to save a printout of the curve. To print
the quench curve, highlight “Add or Delete Quench/Efficiency Pairs” and press SELECT.
With the menu shown in Figure 6.16 displayed, press START. When the quench curve is
printed, press PREVIOUS MENU to display the menu shown in Figure 6.14 again.
7. Highlight “Delete Entire Curve”.
NOTE Before proceeding, ensure that the curve selected and displayed next to “Select Quench Curve:” is the
curve you want to delete. Once the delete action is taken, all the parameters for this curve are lost.
NOTE A curve deleted accidentally can be restored, point by point, from the printout of the original quench
correlation table, if available. Refer to Manual Entry of Quench Curves Section 6 for information on manually
entering a quench curve.
Once you are assured this is the correct quench curve, press DELETE. The curve is deleted.
8. If no further editing is required, highlight “Review/Edit Complete” and press SELECT. If
you are finished using the DPM Library, press MAIN MENU.
Manual Entry of Quench Curves
A quench curve that is no longer stored in the DPM Library can be re-entered If a printout or
other record of the quench curve (H#’s or IC#’s and efficiencies) is available. The curve is
entered by adding each data point and quench monitor value. Five to ten points may be
added.
To manually enter a quench curve:
1. Follow steps 1-12 given in Counting the Standards Section 6, Counting the Standards.
2. Press the Down Cursor Arrow key to display the menu shown in Figure 6.11. Highlight
“Enter Quench Curve Manually” and press SELECT. The menu shown in Figure 6.16 is
displayed. All values are zero.
3. To enter points to the quench curve, type in the H# or IC# value and the % Efficiency for
each point you wish to add. For dual and triple label quench curves, enter values for Eff-
1, Eff-2 and Eff-3. Press ENTER after each value is typed in. Use the Cursor Arrow keys
to move to the next entry. A maximum often points for each quench curve may be
stored.
- LS 6000 Series 1
- Table of Contents 3
- Introduction 11
- Principles of Operation 12
- Operating the Instrument 12
- Operating Modes 13
- 1.3 Specifications 14
- Precautions and Limitations 15
- Figure 1.1 Standard Vial 15
- Miniature Vials 16
- 1.5 Hazards 17
- Maintenance 18
- Getting Started 19
- 2.2 Power Failure 21
- 2.3 Operating Controls 21
- Operator Control Key pad 22
- Using the Operating Controls 24
- 2.4 Using the Racks 25
- Using the Racks 26
- Setting Up the Racks 27
- 2.5 Preparing the Printer 29
- 2.6 System Setup 30
- Energy Scale 31
- Printer Paging 32
- Allow Interrupt Count 32
- System Setup 33
- Figure 2.9 RS232 Setup Menu 33
- Date/Time 35
- Auto DPM 35
- 2.7 Calibration 36
- Counting Samples 39
- Starting the Automatic Count 40
- Conducting Count Single Rack 41
- 3.4 Auto DPM 46
- 3.5 Multi-Task 47
- Interrupt Count in Multi-Task 48
- Multi-Task 50
- Interrupt Data 51
- Setting Up User Programs 59
- 4.2 Editing A User Program 61
- Editing A User Program 62
- Comments 65
- Counting Time 65
- Liquid or Xtal Scintillator 65
- Isotope 1 65
- Isotope 2 and Isotope 3 66
- Edit Other Parameters 67
- Counting Precision 69
- Background/Blank Subtraction 69
- Lum-Ex Correction 71
- Phase Monitor 72
- Low Level 72
- Low Count Reject 72
- Output Formats 72
- Count Data 75
- Raw Data 75
- Collecting Spectral Data 76
- 4.3 Copy User Program 77
- Copy User Program 78
- 5.2 CPM/Xtal CPM 80
- CPM/Xtal CPM 81
- Results for CPM/Xtal CPM 83
- 5.4 Auto DPM 85
- Setting Up Auto DPM 86
- Loading Samples for Auto DPM 86
- Results for Auto DPM 86
- Setting Up DPM 87
- 5.6 Xtal DPM 89
- Xtal DPM 90
- Setting Up Xtal DPM 91
- Loading Samples for Xtal DPM 92
- 5.7 DPM % of Reference 93
- Setting Up DPM % of Reference 94
- Xtal SL DPM % of Reference 95
- 5.9 Single Photon Monitoring 98
- Data Calculation 100
- Single Photon Monitoring 100
- Isotope/DPM Libraries 103
- Accessing the Isotope Library 104
- Printing the Isotope Library 104
- The Isotope Library 105
- Setup Menu 106
- PN 247971-F 108
- 5 minutes 109
- 6.2 Setting Up A Quench Curve 110
- Setting Up A Quench Curve 112
- Counting the Standards 114
- Editing Quench Curves 120
- Deleting A Quench Curve 124
- Manual Entry of Quench Curves 125
- 7.1 Chemiluminescence 127
- Interpretation of Results 128
- Reducing Single Photon Events 128
- 7.3 Two Phase Samples 129
- Procedures 131
- Analysis of Data 131
- H Counting Efficiency 132
- C Counting Efficiency 132
- Background 133
- Contamination 133
- Instrument Specifications 135
- Temperature Control Accessory 138
- Installation Requirements 139
- Electrical Requirements 140
- 0.5 to 1.0 m in 140
- Environment Requirements 142
- . Note that the output 144
- Datum IDs 146
- CHAPTER 1, PART 31 167
- Region I 170
- Region II 170
- Region III 170
- Region IV 170
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