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LS 6000 Scintillation System User’s Manual
PN 247971-F
2-10
Getting Started
Using the Racks
To set up the Calibrate Rack, select one of the standard or miniature racks, depending on the
size of your unquenched standards. If the instrument is ordered as a Miniature Rack System,
the unquenched calibration standards supplied with the instrument are miniature vials. If the
instrument is ordered as a Standard Rack System, the unquenched calibration standards
supplied with the instrument are standard vials. The size of the colored racks matches the size
of the calibration standards.
Install the Auto Calibrate Card as a Command Card. Refer to Installing Cards Section 2
above. Turn the rack around, and place the sealed, unquenched ~ standard in the #1 position
of the rack. Only the first sample in the rack is counted during calibration,
except when
calibrating for Auto DPM. Place
the other two sealed standards in the same rack. Although not used
for calibration, these samples are required for other procedures and this is a useful place to store them.
NOTE The 3H standard is used for calibrating the system for Auto DPM. Refer to Section 2 Auto DPM for
more information on Auto DPM.
Halt Rack
The Halt Rack is a rack bearing the Halt Card. The Halt Rack is placed after the last rack of samples. It
does not contain any samples. The instrument recognizes the Halt Rack and stops counting. Refer to
Section 2.4 for information on using the Halt Rack.
To set up the Halt Rack, select the red rack provided
and insert the Halt Card as a Command Card onto
the rack as described above.
Interrupt Rack
The Interrupt Rack is the rack bearing the Interrupt Card. The Interrupt Rack with the Interrupt Card
installed on it will not be counted during Automatic Count when it is left in the instrument, unless
Interrupt Count is initiated from Multi-Task. Refer to Section 2 Setting Up the Racks for information
on using the Interrupt Rack.
To set up the Interrupt Rack, select the yellow rack and insert the Interrupt Card as a Rack
Number Card onto the rack as described above.
NOTE The Interrupt Rack does not have a Command Card in-stalled. The Interrupt Card is a Rack Number
Card.
Auto DPM Rack
The Auto DPM Rack is a rack bearing the Auto DPM Card. The Auto DPM Rack is used to
initiate the Auto DPM Program. Refer to Section 2 Setting Up the Racks for information on
using the Auto DPM Rack. To set up the Auto DPM Rack, select a miniature or standard vial
rack and insert the Auto DPM Card as a Command Card onto the rack as described above.
Place a Rack Number Card on the rack as described above, if desired.
Sample Racks
Up to 50 different User Programs can be stored in the instrument and called up during
Automatic Count using the User Number Cards 1
— 50. The first rack of each batch of samples
has the appropriate User Number Card installed on it. The first rack and the remaining
Sample Racks can have a Rack Number Card installed on them to provide positive sample
identification. It is convenient to install the User Number Cards and the Rack Number Cards
you anticipate using onto the racks and leaving them there.
- LS 6000 Series 1
- Table of Contents 3
- Introduction 11
- Principles of Operation 12
- Operating the Instrument 12
- Operating Modes 13
- 1.3 Specifications 14
- Precautions and Limitations 15
- Figure 1.1 Standard Vial 15
- Miniature Vials 16
- 1.5 Hazards 17
- Maintenance 18
- Getting Started 19
- 2.2 Power Failure 21
- 2.3 Operating Controls 21
- Operator Control Key pad 22
- Using the Operating Controls 24
- 2.4 Using the Racks 25
- Using the Racks 26
- Setting Up the Racks 27
- 2.5 Preparing the Printer 29
- 2.6 System Setup 30
- Energy Scale 31
- Printer Paging 32
- Allow Interrupt Count 32
- System Setup 33
- Figure 2.9 RS232 Setup Menu 33
- Date/Time 35
- Auto DPM 35
- 2.7 Calibration 36
- Counting Samples 39
- Starting the Automatic Count 40
- Conducting Count Single Rack 41
- 3.4 Auto DPM 46
- 3.5 Multi-Task 47
- Interrupt Count in Multi-Task 48
- Multi-Task 50
- Interrupt Data 51
- Setting Up User Programs 59
- 4.2 Editing A User Program 61
- Editing A User Program 62
- Comments 65
- Counting Time 65
- Liquid or Xtal Scintillator 65
- Isotope 1 65
- Isotope 2 and Isotope 3 66
- Edit Other Parameters 67
- Counting Precision 69
- Background/Blank Subtraction 69
- Lum-Ex Correction 71
- Phase Monitor 72
- Low Level 72
- Low Count Reject 72
- Output Formats 72
- Count Data 75
- Raw Data 75
- Collecting Spectral Data 76
- 4.3 Copy User Program 77
- Copy User Program 78
- 5.2 CPM/Xtal CPM 80
- CPM/Xtal CPM 81
- Results for CPM/Xtal CPM 83
- 5.4 Auto DPM 85
- Setting Up Auto DPM 86
- Loading Samples for Auto DPM 86
- Results for Auto DPM 86
- Setting Up DPM 87
- 5.6 Xtal DPM 89
- Xtal DPM 90
- Setting Up Xtal DPM 91
- Loading Samples for Xtal DPM 92
- 5.7 DPM % of Reference 93
- Setting Up DPM % of Reference 94
- Xtal SL DPM % of Reference 95
- 5.9 Single Photon Monitoring 98
- Data Calculation 100
- Single Photon Monitoring 100
- Isotope/DPM Libraries 103
- Accessing the Isotope Library 104
- Printing the Isotope Library 104
- The Isotope Library 105
- Setup Menu 106
- PN 247971-F 108
- 5 minutes 109
- 6.2 Setting Up A Quench Curve 110
- Setting Up A Quench Curve 112
- Counting the Standards 114
- Editing Quench Curves 120
- Deleting A Quench Curve 124
- Manual Entry of Quench Curves 125
- 7.1 Chemiluminescence 127
- Interpretation of Results 128
- Reducing Single Photon Events 128
- 7.3 Two Phase Samples 129
- Procedures 131
- Analysis of Data 131
- H Counting Efficiency 132
- C Counting Efficiency 132
- Background 133
- Contamination 133
- Instrument Specifications 135
- Temperature Control Accessory 138
- Installation Requirements 139
- Electrical Requirements 140
- 0.5 to 1.0 m in 140
- Environment Requirements 142
- . Note that the output 144
- Datum IDs 146
- CHAPTER 1, PART 31 167
- Region I 170
- Region II 170
- Region III 170
- Region IV 170
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